Structures by: Nayak P. S.

Total: 52

<i>N</i>-(4-Chloro-3-methylphenyl)-2-phenylacetamide

C15H14ClNO

Nayak, Prakash S.Jasinski, Jerry P.Golen, James A.Narayana, BadiadkaKaur, ManpreetYathirajan, Hemmige S.Glidewell, Christopher

Acta crystallographica. Section C, Structural chemistry (2014) 70, Pt 9 889-894

a=5.0039(7)Å   b=10.7525(12)Å   c=12.6177(12)Å

α=108.615(10)°   β=91.771(11)°   γ=90.167(11)°

<i>N</i>-(4-Chloro-3-methylphenyl)-2-(2,4-dichlorophenyl)acetamide

C15H12Cl3NO

Nayak, Prakash S.Jasinski, Jerry P.Golen, James A.Narayana, BadiadkaKaur, ManpreetYathirajan, Hemmige S.Glidewell, Christopher

Acta crystallographica. Section C, Structural chemistry (2014) 70, Pt 9 889-894

a=11.8441(7)Å   b=4.7288(3)Å   c=13.0981(7)Å

α=90°   β=101.310(6)°   γ=90°

<i>N</i>-(4-Bromo-3-methylphenyl)-2-(2-chlorophenyl)acetamide

C15H13BrClNO

Nayak, Prakash S.Jasinski, Jerry P.Golen, James A.Narayana, BadiadkaKaur, ManpreetYathirajan, Hemmige S.Glidewell, Christopher

Acta crystallographica. Section C, Structural chemistry (2014) 70, Pt 9 889-894

a=11.8458(8)Å   b=4.7282(3)Å   c=25.0757(15)Å

α=90°   β=98.133(5)°   γ=90°

(2<i>E</i>)-3-(6-Methoxynaphthalen-2-yl)-1-(pyridin-3-yl)prop-2-en-1-one

C19H15NO2

Nayak, Prakash S.Narayana, BadiadkaYathirajan, Hemmige S.Hosten, Eric C.Betz, RichardGlidewell, Christopher

Acta Crystallographica Section C (2014) 70, 11 1011-1016

a=14.2636(6)Å   b=16.6789(6)Å   c=6.0084(2)Å

α=90°   β=90°   γ=90°

(<i>RS</i>)-2-Amino-4-(6-methoxynaphthalen-2-yl)-6-(pyridin-3-yl)-3,4-dihydropyrimidine monohydrate

C20H18N4O,H2O

Nayak, Prakash S.Narayana, BadiadkaYathirajan, Hemmige S.Hosten, Eric C.Betz, RichardGlidewell, Christopher

Acta Crystallographica Section C (2014) 70, 11 1011-1016

a=17.2244(5)Å   b=5.9552(2)Å   c=18.5173(6)Å

α=90°   β=112.8300(10)°   γ=90°

2-(4-Chlorophenyl)-6-methoxychroman-4-one

C16H13ClO3

Jasinski, Jerry P.Pek, Albert E.Narayana, B.Yathirajan, H. S.Nayak, Prakash S.

Acta Crystallographica Section E (2010) 66, 10 o2546-o2547

a=5.0188(3)Å   b=12.0138(7)Å   c=12.3708(7)Å

α=108.035(5)°   β=98.379(4)°   γ=91.820(5)°

(<i>E</i>)-3-(4-Methoxyphenyl)-1-[4-(piperidin-1-yl)phenyl]prop-2-en-1-one

C21H23NO2

Jasinski, Jerry P.Guild, Curtis J.Narayana, B.Nayak, Prakash S.Yathirajan, H. S.

Acta Crystallographica Section E (2010) 66, 8 o1996

a=6.0963(11)Å   b=10.985(2)Å   c=13.133(3)Å

α=74.188(3)°   β=88.674(3)°   γ=77.393(3)°

1-(10<i>H</i>-Phenothiazin-2-yl)ethanone

C14H11NOS

Jasinski, Jerry P.Pek, Albert E.Nayak, Prakash S.Narayana, B.Yathirajan, H. S.

Acta Crystallographica Section E (2011) 67, 2 o430-o431

a=14.3445(18)Å   b=5.5425(7)Å   c=15.694(2)Å

α=90.00°   β=114.494(2)°   γ=90.00°

<i>N</i>-(4-Bromophenyl)-2-(naphthalen-1-yl)acetamide

C18H14BrNO

Fun, Hoong-KunQuah, Ching KhengNarayana, B.Nayak, Prakash S.Sarojini, B. K.

Acta Crystallographica Section E (2011) 67, 11 o2926-o2927

a=12.6837(11)Å   b=9.4047(11)Å   c=25.641(3)Å

α=90.00°   β=90.00°   γ=90.00°

(2<i>E</i>)-1-(2,5-Dimethoxyphenyl)-3-(3-nitrophenyl)prop-2-en-1-one

C17H15NO5

Fun, Hoong-KunChia, Tze ShyangNarayana, B.Nayak, Prakash S.Sarojini, B. K.

Acta Crystallographica Section E (2011) 67, 11 o3058-o3059

a=7.5015(5)Å   b=7.9962(5)Å   c=13.2468(8)Å

α=86.5070(10)°   β=80.3420(10)°   γ=76.3320(10)°

<i>N</i>-(3,5-Dichlorophenyl)-2-(naphthalen-1-yl)acetamide

C18H13Cl2NO

Fun, Hoong-KunQuah, Ching KhengNarayana, B.Nayak, Prakash S.Sarojini, B. K.

Acta Crystallographica Section E (2011) 67, 11 o2941-o2942

a=7.8090(14)Å   b=24.811(4)Å   c=9.6783(13)Å

α=90.00°   β=125.050(10)°   γ=90.00°

<i>N</i>-(4-Bromophenyl)-2-(4-chlorophenyl)acetamide

C14H11BrClNO

Fun, Hoong-KunShahani, TaraNayak, Prakash S.Narayana, B.Sarojini, B. K.

Acta Crystallographica Section E (2012) 68, 2 o519

a=15.584(8)Å   b=4.763(3)Å   c=18.139(10)Å

α=90.00°   β=96.984(11)°   γ=90.00°

(2<i>E</i>)-1-(3,4-Dichlorophenyl)-3-(2-hydroxyphenyl)prop-2-en-1-one

C15H10Cl2O2

Jasinski, Jerry P.Golen, James A.Nayak, Prakash S.Narayana, B.Yathirajan, H. S.

Acta Crystallographica Section E (2012) 68, 2 o366

a=7.2551(6)Å   b=7.8351(7)Å   c=12.8049(11)Å

α=92.367(7)°   β=102.946(8)°   γ=109.011(8)°

2-(4-Bromophenyl)-<i>N</i>-(pyrazin-2-yl)acetamide

C12H10BrN3O

Nayak, Prakash S.Narayana, B.Jasinski, Jerry P.Yathirajan, H. S.Sarojini, B. K.

Acta Crystallographica Section E (2013) 69, 6 o891

a=10.6804(4)Å   b=7.5196(3)Å   c=29.1355(10)Å

α=90°   β=90°   γ=90°

<i>N</i>-(1,3-Benzothiazol-2-yl)acetamide

C9H8N2OS

Nayak, Prakash S.Narayana, B.Jasinski, Jerry P.Yathirajan, H. S.Kaur, Manpreet

Acta Crystallographica Section E (2013) 69, 11 o1622

a=11.1852(4)Å   b=7.4037(4)Å   c=20.9189(8)Å

α=90°   β=94.408(3)°   γ=90°

<i>N</i>-(2,4-Dimethylphenyl)-2,2-diphenylacetamide

C22H21NO

Fun, Hoong-KunChia, Tze ShyangNayak, Prakash S.Narayana, B.Sarojini, B. K.

Acta Crystallographica Section E (2012) 68, 5 o1316-o1317

a=9.5520(9)Å   b=10.2011(10)Å   c=17.9656(17)Å

α=91.030(2)°   β=98.957(2)°   γ=90.377(2)°

2-(2,4-Dichlorophenyl)-<i>N</i>-(1,5-dimethyl-3-oxo-2-phenyl-2,3-dihydro- 1<i>H</i>-pyrazol-4-yl)acetamide

C19H17Cl2N3O2

Butcher, Ray J.Mahan, AneekaNayak, P. S.Narayana, B.Yathirajan, H. S.

Acta Crystallographica Section E (2013) 69, 1 o39

a=25.1853(5)Å   b=8.18108(9)Å   c=21.0978(4)Å

α=90.00°   β=119.772(3)°   γ=90.00°

4-(4-Iodoanilino)-2-methylene-4-oxobutanoic acid

C11H10INO3

Nayak, Prakash S.Narayana, BadiadkaYathirajan, Hemmige S.Gerber, Thomasvan Brecht, BenjaminBetz, Richard

Acta Crystallographica Section E (2013) 69, 1 o83

a=23.1111(6)Å   b=4.78630(10)Å   c=10.4262(2)Å

α=90.00°   β=97.0710(10)°   γ=90.00°

2-(2,6-Dichlorophenyl)-<i>N</i>-(1,5-dimethyl-3-oxo-2-phenyl-2,3-dihydro- 1<i>H</i>-pyrazol-4-yl)acetamide

C19H17Cl2N3O2

Butcher, Ray J.Mahan, AneekaNayak, P. S.Narayana, B.Yathirajan, H. S.

Acta Crystallographica Section E (2013) 69, 1 o46-o47

a=20.3442(11)Å   b=12.1080(8)Å   c=14.9500(8)Å

α=90.00°   β=93.837(5)°   γ=90.00°

4-[(<i>E</i>)-(4-Benzyloxybenzylidene)amino]-1,5-dimethyl-2-phenyl- 1<i>H</i>-pyrazol-3(2<i>H</i>)-one

C25H23N3O2

Kant, RajniGupta, Vivek K.Kapoor, KaminiNayak, Prakash S.Sarojini, B. K.Narayana, B.

Acta Crystallographica Section E (2013) 69, 1 o115

a=13.0079(5)Å   b=9.9079(4)Å   c=17.0469(9)Å

α=90.00°   β=103.674(4)°   γ=90.00°

2-(2-Methylphenyl)-<i>N</i>-(1,3-thiazol-2-yl)acetamide

C12H12N2OS

Narayana, B.Nayak, Prakash S.Sarojini, Balladka K.Jasinski, Jerry P.

Acta Crystallographica Section E (2014) 70, 6 o716

a=17.6983(6)Å   b=4.94078(13)Å   c=14.4603(5)Å

α=90°   β=111.236(4)°   γ=90°

4-[(4-Acetylphenyl)amino]-2-methylidene-4-oxobutanoic acid

C13H13NO4

Narayana, B.Nayak, Prakash S.Sarojini, Balladka K.Jasinski, Jerry P.

Acta Crystallographica Section E (2014) 70, 7 o752-o753

a=5.0164(5)Å   b=5.2908(4)Å   c=21.8464(18)Å

α=92.833(6)°   β=90.315(7)°   γ=96.222(7)°

4-[(4-Bromophenyl)amino]-2-methylidene-4-oxobutanoic acid

C11H10BrNO3

Narayana, B.Nayak, Prakash S.Sarojini, Balladka K.Jasinski, Jerry P.

Acta Crystallographica Section E (2014) 70, 7 o779-o780

a=6.2782(4)Å   b=8.3251(5)Å   c=21.3244(12)Å

α=96.462(5)°   β=92.026(5)°   γ=95.390(5)°

(2<i>E</i>)-3-(3-Nitrophenyl)-1-[4-(piperidin-1-yl)phenyl]prop-2-en-1-one

C20H20N2O3

Fun, Hoong-KunChia, Tze ShyangNayak, Prakash S.Narayana, B.Sarojini, B. K.

Acta Crystallographica Section E (2012) 68, 4 o974

a=7.4268(12)Å   b=11.3884(18)Å   c=39.447(6)Å

α=90.00°   β=90.00°   γ=90.00°

<i>N</i>-(2,6-Dichlorophenyl)-2-(naphthalen-1-yl)acetamide

C18H13Cl2NO

Fun, Hoong-KunQuah, Ching KhengNayak, Prakash S.Narayana, B.Sarojini, B. K.

Acta Crystallographica Section E (2012) 68, 5 o1385

a=13.1918(13)Å   b=4.7199(5)Å   c=24.878(2)Å

α=90.00°   β=103.127(3)°   γ=90.00°

<i>N</i>-(2,6-Dimethylphenyl)-2,2-diphenylacetamide

C22H21NO

Fun, Hoong-KunChia, Tze ShyangNayak, Prakash S.Narayana, B.Sarojini, B. K.

Acta Crystallographica Section E (2012) 68, 5 o1287-o1288

a=12.0606(10)Å   b=16.6747(13)Å   c=8.9469(7)Å

α=90.00°   β=108.080(2)°   γ=90.00°

2,2-Diphenyl-<i>N</i>-(1,3-thiazol-2-yl)acetamide

C17H14N2OS

Fun, Hoong-KunOoi, Chin WeiNayak, Prakash S.Narayana, B.Sarojini, B. K.

Acta Crystallographica Section E (2012) 68, 5 o1312-o1313

a=5.69150(10)Å   b=15.1889(2)Å   c=16.5967(2)Å

α=90.00°   β=97.8450(10)°   γ=90.00°

<i>N</i>-(3,4-Difluorophenyl)-2,2-diphenylacetamide

C20H15F2NO

Fun, Hoong-KunOoi, Chin WeiNayak, Prakash S.Narayana, B.Sarojini, B. K.

Acta Crystallographica Section E (2012) 68, 5 o1349-o1350

a=9.9756(2)Å   b=18.0181(3)Å   c=9.8107(2)Å

α=90.00°   β=117.0640(10)°   γ=90.00°

<i>N</i>-(1,3-Thiazol-2-yl)-2-(2,4,6-trimethylphenyl)acetamide

C14H16N2OS

Fun, Hoong-KunQuah, Ching KhengNayak, Prakash S.Narayana, B.Sarojini, B. K.

Acta Crystallographica Section E (2012) 68, 8 o2461

a=16.421(2)Å   b=4.6397(7)Å   c=20.1144(18)Å

α=90.00°   β=123.150(7)°   γ=90.00°

1-(3-Bromophenyl)thiourea

C7H7BrN2S

Fun, Hoong-KunQuah, Ching KhengNayak, Prakash S.Narayana, B.Sarojini, B. K.

Acta Crystallographica Section E (2012) 68, 8 o2462

a=5.5308(8)Å   b=8.5316(12)Å   c=9.4249(14)Å

α=103.500(3)°   β=90.878(3)°   γ=97.232(4)°

<i>N</i>-(4-Chlorophenyl)-2-(naphthalen-1-yl)acetamide

C18H14ClNO

Fun, Hoong-KunQuah, Ching KhengNayak, Prakash S.Narayana, B.Sarojini, B. K.

Acta Crystallographica Section E (2012) 68, 8 o2463

a=19.163(6)Å   b=5.0458(11)Å   c=17.252(4)Å

α=90.00°   β=116.365(5)°   γ=90.00°

2-(Naphthalen-1-yl)-<i>N</i>-(1,3-thiazol-2-yl)acetamide

C15H12N2OS

Fun, Hoong-KunQuah, Ching KhengNayak, Prakash S.Narayana, B.Sarojini, B. K.

Acta Crystallographica Section E (2012) 68, 8 o2464

a=5.26680(10)Å   b=13.0861(2)Å   c=18.5373(3)Å

α=90.00°   β=105.6400(10)°   γ=90.00°

2-(4-Bromophenyl)-<i>N</i>-(5-methylpyridin-2-yl)acetamide

C14H13BrN2O

Fun, Hoong-KunOoi, Chin WeiNayak, Prakash S.Narayana, B.Sarojini, B. K.

Acta Crystallographica Section E (2012) 68, 8 o2526

a=14.0086(16)Å   b=9.4215(11)Å   c=20.610(2)Å

α=90.00°   β=109.040(2)°   γ=90.00°

1-(3-Chlorophenyl)thiourea

C7H7ClN2S

Fun, Hoong-KunQuah, Ching KhengNayak, Prakash S.Narayana, B.Sarojini, B. K.

Acta Crystallographica Section E (2012) 68, 8 o2423

a=5.4406(3)Å   b=8.5715(4)Å   c=9.2392(4)Å

α=104.221(2)°   β=91.776(2)°   γ=96.362(2)°

1-(2,4-Difluorophenyl)thiourea

C7H6F2N2S

Fun, Hoong-KunQuah, Ching KhengNayak, Prakash S.Narayana, B.Sarojini, B. K.

Acta Crystallographica Section E (2012) 68, 8 o2460

a=6.4260(7)Å   b=36.908(4)Å   c=6.6821(7)Å

α=90.00°   β=100.464(2)°   γ=90.00°

2-(2-Fluorophenyl)-<i>N</i>-(1,3-thiazol-2-yl)acetamide

C11H9FN2OS

Fun, Hoong-KunQuah, Ching KhengNayak, Prakash S.Narayana, B.Sarojini, B. K.

Acta Crystallographica Section E (2012) 68, 8 o2565

a=11.9043(13)Å   b=5.2969(6)Å   c=16.4579(18)Å

α=90.00°   β=90.397(3)°   γ=90.00°

2-(4-Bromophenyl)-<i>N</i>-(3-chloro-4-fluorophenyl)acetamide

C14H10BrClFNO

Fun, Hoong-KunQuah, Ching KhengNayak, Prakash S.Narayana, B.Sarojini, B. K.

Acta Crystallographica Section E (2012) 68, 8 o2558

a=4.9120(5)Å   b=6.3131(6)Å   c=42.517(4)Å

α=90.00°   β=90.00°   γ=90.00°

<i>N</i>-(4-Chlorophenyl)-2,2-diphenylacetamide

C20H16ClNO

Fun, Hoong-KunLoh, Wan-SinNayak, Prakash S.Narayana, B.Sarojini, B. K.

Acta Crystallographica Section E (2012) 68, 8 o2556-o2557

a=10.2147(2)Å   b=17.8203(4)Å   c=9.5730(2)Å

α=90.00°   β=114.0190(10)°   γ=90.00°

(2<i>E</i>)-3-(2-Fluorophenyl)-1-(4-fluorophenyl)prop-2-en-1-one

C15H10F2O

Fun, Hoong-KunFarhadikoutenaei, AbbasNarayana, B.Nayak, Prakash S.Sarojini, B. K.

Acta Crystallographica Section E (2012) 68, 9 o2658

a=14.569(2)Å   b=7.2737(10)Å   c=11.3933(15)Å

α=90.00°   β=108.827(3)°   γ=90.00°

<i>N</i>-(2-Bromophenyl)-2-(naphthalen-1-yl)acetamide

C18H14BrNO

Fun, Hoong-KunQuah, Ching KhengNayak, Prakash S.Narayana, B.Sarojini, B. K.

Acta Crystallographica Section E (2012) 68, 9 o2657

a=4.76030(10)Å   b=11.4614(3)Å   c=26.6255(6)Å

α=90.00°   β=90.00°   γ=90.00°

2,2-Diphenyl-<i>N</i>-(2,4,5-trichlorophenyl)acetamide

C20H14Cl3NO

Fun, Hoong-KunQuah, Ching KhengNayak, Prakash S.Narayana, B.Sarojini, B. K.

Acta Crystallographica Section E (2012) 68, 9 o2659-o2660

a=18.6630(16)Å   b=17.1713(15)Å   c=22.5648(19)Å

α=90.00°   β=90.00°   γ=90.00°

2-(4-Chlorophenyl)-<i>N</i>-(1,3-thiazol-2-yl)acetamide

C11H9ClN2OS

Fun, Hoong-KunQuah, Ching KhengNayak, Prakash S.Narayana, B.Sarojini, B. K.

Acta Crystallographica Section E (2012) 68, 9 o2679

a=13.9169(13)Å   b=5.5188(5)Å   c=15.1836(14)Å

α=90.00°   β=100.311(2)°   γ=90.00°

2-(4-Bromophenyl)-<i>N</i>-(2,6-dimethylphenyl)acetamide

C16H16BrNO

Fun, Hoong-KunQuah, Ching KhengNayak, Prakash S.Narayana, B.Sarojini, B. K.

Acta Crystallographica Section E (2012) 68, 9 o2678

a=4.7146(6)Å   b=22.999(3)Å   c=13.5350(15)Å

α=90.00°   β=91.138(3)°   γ=90.00°

<i>N</i>-(1,5-Dimethyl-3-oxo-2-phenyl-2,3-dihydro-1<i>H</i>-pyrazol-4-yl)- 2-[4-(methylsulfanyl)phenyl]acetamide

C20H21N3O2S

Fun, Hoong-KunQuah, Ching KhengNayak, Prakash S.Narayana, B.Sarojini, B. K.

Acta Crystallographica Section E (2012) 68, 9 o2677

a=14.9176(8)Å   b=6.6527(4)Å   c=19.5792(10)Å

α=90.00°   β=110.6890(10)°   γ=90.00°

(2<i>E</i>)-3-[4-(Benzyloxy)phenyl]-1-(pyridin-3-yl)prop-2-en-1-one

C21H17NO2

Fun, Hoong-KunQuah, Ching KhengNayak, Prakash S.Narayana, B.Sarojini, B. K.

Acta Crystallographica Section E (2012) 68, 9 o2724

a=5.9845(6)Å   b=38.187(4)Å   c=8.5412(7)Å

α=90.00°   β=123.372(5)°   γ=90.00°

1,1'-[2,4-Bis(3-nitrophenyl)cyclobutane-1,3-diyl]diphenylmethanone

C30H22N2O6

Nayak, Prakash S.Narayana, BadiadkaYathirajan, Hemmige S.Gerber, ThomasHosten, EricBetz, Richard

Acta Crystallographica Section E (2012) 68, 12 o3272-o3273

a=5.78500(10)Å   b=14.7824(3)Å   c=14.3589(3)Å

α=90.00°   β=104.8580(10)°   γ=90.00°

2-(3,4-Dichlorophenyl)-<i>N</i>-(1,5-dimethyl-3-oxo-2-phenyl-2,3-dihydro- 1<i>H</i>-pyrazol-4-yl)acetamide

C19H17Cl2N3O2

Mahan, AneekaButcher, Ray J.Nayak, Prakash S.Narayana, B.Yathirajan, H. S.

Acta Crystallographica Section E (2013) 69, 3 o402-o403

a=17.2064(8)Å   b=20.7984(9)Å   c=15.6102(7)Å

α=90.00°   β=101.213(4)°   γ=90.00°

2-(2,6-Dichlorophenyl)-<i>N</i>-(1,3-thiazol-2-yl)acetamide

C11H8Cl2N2OS

Nayak, Prakash S.Narayana, B.Yathirajan, H. S.Jasinski, Jerry P.Butcher, Ray J.

Acta Crystallographica Section E (2013) 69, 4 o523

a=7.1278(4)Å   b=8.4434(4)Å   c=10.3637(6)Å

α=95.341(4)°   β=106.140(5)°   γ=96.745(4)°

2-(3,4-Dichlorophenyl)-<i>N</i>-(1,3-thiazol-2-yl)acetamide

C11H8Cl2N2OS

Nayak, Prakash S.Narayana, B.Yathirajan, H. S.Jasinski, Jerry P.Butcher, Ray J.

Acta Crystallographica Section E (2013) 69, 5 o645-o646

a=4.6185(3)Å   b=7.7741(7)Å   c=17.1188(12)Å

α=100.278(7)°   β=94.250(6)°   γ=105.001(7)°

2-(2,4-Dichlorophenyl)-<i>N</i>-(1,3-thiazol-2-yl)acetamide

C11H8Cl2N2OS

Nayak, Prakash S.Narayana, B.Yathirajan, H. S.Jasinski, Jerry P.Butcher, Ray J.

Acta Crystallographica Section E (2013) 69, 5 o656-o657

a=5.3262(2)Å   b=10.5083(4)Å   c=10.8096(4)Å

α=83.900(3)°   β=86.301(3)°   γ=87.279(4)°

4-(3-Fluoro-4-methylanilino)-2-methylidene-4-oxobutanoic acid

C12H12FNO3

Nayak, Prakash S.Narayana, B.Jasinski, Jerry P.Yathirajan, H. S.Kaur, Manpreet

Acta Crystallographica Section E (2013) 69, 12 o1752

a=6.3368(3)Å   b=8.2642(4)Å   c=21.0277(11)Å

α=84.057(4)°   β=89.798(4)°   γ=86.062(4)°

<i>N</i>-(4-Bromo-3-methylphenyl)-2-phenylacetamide

C15H14BrNO

Nayak, Prakash S.Jasinski, Jerry P.Golen, James A.Narayana, BadiadkaKaur, ManpreetYathirajan, Hemmige S.Glidewell, Christopher

Acta crystallographica. Section C, Structural chemistry (2014) 70, Pt 9 889-894

a=4.9995(3)Å   b=10.8392(4)Å   c=12.7301(7)Å

α=108.149(4)°   β=91.968(5)°   γ=90.310(4)°